- 期刊
蔬菜中加保扶(Carbofuran)殘留量檢驗方法之檢討
Studies on the Method of Pesticide Residue Analysis for Carbofuran in Vegetables
摘要
以Trifluoroacetylation方法使加保抉(Carbofuran)農藥得以用ECD為檢出器之氣相層析儀中分析，其感度為1ng，但在整個分析過程中以淨化過程之矽膠鎂使用量應保持在7~8g之間，淨化管管徑在1.0~1.2cm間，則其回收率可得80.4~91.6%。然而高回收率之條件並不適於所有之檢體，因為雜質可能干擾氣相層析圖譜之分析，故應視不同之檢體選擇過當之條件。
關鍵字
無資料並列摘要
Using trifluoroacetylation determination of carbofuran residue with GC-ECD was studied. The recovery was between 80.3-91.6% and the detectability was 1 ng. The key point to getting high recovery, the strict work on florisil column was required. The amount of florisil, inside diameter of column and eluant would influence the carbofuran elution. Seven to eight grams of florisil, 1.0-1.2cm inside diameter and ethyl ether: n-hexane (1:9) as an eluant were perforemed sufficiently for analysis. The method showed high recovery and reproducibility.
延伸閱讀
- 張美惠、賴昭伶、李苹苹、鄭秋真、周薰修（1990）。多重殘留分析法於蔬菜中殘留農藥之偵測。藥物食品檢驗局調查研究年報，()，236-246。https://doi.org/10.6946/ASRNL.199009.0236
- Sheu, C., & Chen, H. C. (2009). 以液相層析檢測蔬果中巨環內酯類農藥之殘留. 藥物食品分析, 17(3), 198-208. https://www.airitilibrary.com/Article/Detail?DocID=10219498-200906-200907150041-200907150041-198-208
- Cheng, C. L., Shih, S. J., Yen, G. C., Chou, S. S., & Liu, C. H. (1994). 以氣相層析／質譜分析法建立蔬果中農藥之多重殘留量檢驗方法. 藥物食品分析, 2(2), 113-122. https://www.airitilibrary.com/Article/Detail?DocID=10219498-199406-2-2-113-122-a
- 周薰修、施淑娟（1995）。應用酵素測試片分析蔬果中的殘留農藥。藥物食品檢驗局調查研究年報，()，89-98。https://doi.org/10.6946/ASRNL.199509.0089
- 溫惠琴、林紹竹、沈孜徽、李婉媜、張碧秋、蔡玉雲、林阿洋、徐錦豐、周薰修（2001）。Monitoring the Contents of Pesticide Residues in Marketed Vegetables and Fruits。藥物食品檢驗局調查研究年報，()，196-208。https://doi.org/10.6946/ASRNL.200109.0196