利用氣相液相層析分離鑑別Morphine, Heroin, Lodeine Phosphate, Pentazocine等成分

Determination of Morphine, Heroin, Lodeine Phosphate, and Pentazocine by Gas Chromatography and High Performance Liquid Chromatography

林澄琴(Cheng-Chin Lin) ； 林春惠(Chung-Hwei Lin) ； 徐廷光(Ting-Guang Shyu) ； 荘清堯(Ching-Yao Chuang)

《藥物食品檢驗局調查研究年報》 5號 (1987/09) Pp. 192-193

https://doi.org/10.6946/ASRNL.198709.0192

並列摘要

For now, TLC is the generally used method for the separation and identification of opium drugs. In this report, we used both GC and HPLC to separate and identify morphine HCl, Heroin, Codeine phosphate and pentazocine. The performance is good and efficient. 3% SE-30 and ov-17, 180 cm×2 mm ID glass tubing, FID and 230℃ were applied for the GC experiment while the experimental conditions for HPLC were (1). column: μ-Bondapak C18; (2). Mobile phase: 5.8 g sodium Dioctyl-Sulfosuccinate in Methanol: Tetrahydrofuran: water=650ml: 20ml: 330ml; (3). UV detector at 280nm; (4). flow rate: 1.5ml/min.