摘要
以電子捕獲式檢出器之氣相層析儀檢測市售人參、當歸、地黃、大棗中藥村中之有機氣農藥之殘留量。其檢測項目包括α-BHC、β-BHC、γ-BHC、pp'-DDT、Aldrin、Dieldrin、Heptachlor 、Endrin、Heptachlor epoxide等九種。以本分析方法，檢測該九種有機氣農藥，其最低檢出限量分別為：α-BHC 9.0 ppb、β-BHC 10.0 ppb、γ-BHC 12.0 ppb、pp'-DDT 15.0 ppb、Aldrin 9.0 ppb、Dieldrin 11.0 ppb、Heptachlor 11.0 ppb、Endrin 12.0 ppb、Heptachlor epoxide 11.0 ppb。其添加回收率介於85.5~91.3%之間。經本分析方法檢測，一百件檢體均未檢出上述九種有機氯農藥。
並列摘要
In this survey, nine kinds of pesticide residuls in 100 samples of marketed Chinese herbs including Ginseng Radix, Angelicae Radix, Rehmanniae Radix and Zizyphi Fructus were carried out by GC/ECD. Nine organic chlorinated pesticides (α-BHC, β-BHC, γ-BHC, Heptachlor, Aldrin, Heptachlor epoxide, Dieldrin, Endrin, pp'-DDT) were investigated. The detection limits of this method were 9.0 ppb for α-BHC, 10.0 ppb for β-BHC, 12.0 ppb for γ-BHC, 11.0 ppb for Heptachlor, 9.0 ppb for Aidrin, 11.0 ppb for Heptachior epoxide, 11.0 ppb for Dieldrin, 12.0 ppb for Endrin, and 15.0 ppb for pp’-DDT. The recoveries were 86.9-88.2% for α-BHC, 85.8~86.5% for β-BHC, 85.9~86.5% for γ-BHC, 88.3~89.4% for Heptachlor, 87.6~89.4% for Aidrin, 89.4~90.7% for Heptachlor epoxide, 89.5~91.3% for Dieldrin, 86.5~91.l% for Endrin, and 87.3~90.0% for pp'-DDT. None of the one hundred herbal samples collected randomly from Chinese herb shops in Taipei City were found to have contained any of the above mentioned.
並列關鍵字
無資料延伸閱讀
- 劉芳淑、曾信雄、溫國慶（1998）。中藥材中殘留農藥之調查(Ⅲ)。藥物食品檢驗局調查研究年報，()，63-74。https://doi.org/10.6946/ASRNL.199809.0063
- 周薰修（1984）。蔬菜中常用農藥之殘留調查研究。藥物食品檢驗局調查研究年報，()，92-96。https://doi.org/10.6946/ASRNL.198409.0092
- 胡智強、徐佩鈴、劉小菁、張雯麗、蔡淑美、蔡慧真、郭曉文、林宜蓉、施鈞傑、周秀冠（2011）。中部地區市售農產品殘留農藥監測。食品藥物研究年報，(2)，124-144。https://doi.org/10.6945/ARFDR.201112.0126
- 徐珮鈴、劉小菁、張雯麗、蔡慧真、蔡淑美、胡智強、陳信志、林宜蓉、陳瑤瓊、周秀冠（2010）。中部地區市售農產品殘留農藥監測。食品藥物研究年報，(1)，52-71。https://doi.org/10.6945/ARFDR.201011.0052
- 劉芳淑、徐雅慧、林宜蓉、賴齡、周令玫、羅吉方、張憲昌、林哲輝（2002）。Investigation of the Quality of Chinese Herbs (Ⅴ)。藥物食品檢驗局調查研究年報，()，162-177。https://doi.org/10.6946/ASRNL.200209.0162