In order to solve the problems of low accuracy and single measuring position in the current method for measuring the flow field characteristics of A^2/O reactor, a laser method for measuring the flow field characteristics of liquid phase in A^2/O reactor was proposed. The system of laser and CCD camera was used to capture the particle displacement in A^2/O reactor at different time periods. The camera divides the captured particle image into several zones, each of which generates the corresponding particle displacement vector. Then, the sub-pixel interpolation method is used to measure the particle velocity in A^2/O reactor to improve the measurement accuracy. The experimental results show that the proposed method can accurately measure the flow characteristics of the internal flow field in A^2/O reactor, and has the advantages of wide detection position, transient and high accuracy.