In this thesis, we investigated the viscosity coefficient of liquid crystal (LC) - E7, with its temperature dependence. In the experiment, we used the polarizing optical microscopy (POM) and Differential Scanning Calorimeter (DSC) to monitor the transition process of liquid crystal. To study the transient behavior of E7, we used the Cone and Plate Viscosmeter to measure the temperature-dependent viscosity coefficient. The POM experimental results show that the phase transition of E7 is a continuous and nonhomogeneous phenomenon depending on the temperature. According to the result, we could analyze the relationship of viscosity coefficient and temperature by calculating the volume ratio in the different states. We found the there is a window for phase transition process of E7, but not a critical temperature point. This result is a new finding and different from any previous investigations. This research will give important information to the fundamental understanding of the phase transition of LC.