Title

Comparison of Extraction Techniques with Different Solvents for DDT Analogues in Sediments

Authors

Yin-Hai Lang;Xin Jiang;D. Martens;Qi-Guo Zhao

Key Words

DDT analogues ; extraction techniques ; sediment ; solvents

PublicationName

PEDOSPHERE(土壤圈)

Volume or Term/Year and Month of Publication

15卷5期(2005 / 10 / 01)

Page #

628 - 633

Content Language

英文

English Abstract

Four techniques, Soxhlet extraction (SOX), ultrasonic extraction (USE), fluidized-bed extraction (FBE) and accelerated solvent extraction (ASE) with different solvents (methanol, hexane/acetone and acetonitrile) were used for the extraction of DDT analogues in sediments. Results revealed that the four extraction techniques had high recoveries (>86.0%) with low standard deviations (<12.0%) for most of DDT analogues, meaning that they could all successfully extract DDT analogues in sediments. Accelerated solvent extraction using methanol and hexane/acetone (1:1), fluidized-bed extraction using hexane/acetone (1:1) and the ultrasonic extraction using hexane/acetone (1:1) were comparable or better than Soxhlet extraction using hexane/acetone (1:1). Considering solvent- and time-consumption, level of automation, and environmental risk, accelerated solvent extraction with hexane/acetone (1:1) was better than the other extraction techniques.

Topic Category 生物農學 > 農業
生物農學 > 森林
生物農學 > 畜牧
生物農學 > 漁業
生物農學 > 生物環境與多樣性