Title

不同形態之鋁粉之燃燒合成氮化鋁粉體之製程開發

Translated Titles

Process Development for Combustion Synthesis of AlN Powder Using Al Reactant with Different Morphology

Authors

林靜欣

Key Words

氮化鋁 ; 燃燒合成法 ; Aluminum Nitride ; Combustion synthesis

PublicationName

成功大學化學工程學系學位論文

Volume or Term/Year and Month of Publication

2010年

Academic Degree Category

碩士

Advisor

鍾賢龍

Content Language

繁體中文

Chinese Abstract

本論文研究是以開發不同形態之鋁粉進行氮化鋁粉體合成。實驗反應物是使用不同於原先實驗室使用的鋁粉,使用的原料為A-2及A-3。 A-2:使用的原料為尺寸75 μm之片狀鋁粉,以恆溫恆濕機作鋁粉表面處理,引燃後通入空氣,在適當反應條件下合成之氮化鋁產物,轉化率在99 %以上。 A-3: 15 ~ 85 μm灰色不規則顆粒狀鋁粉,以均混氮化鋁合成之產物,其轉化率約97.97 %。 本實驗室中所使用的氮化鋁粉體表面改質劑為APS、GPS及磷酸,對其ESCA圖進行分析,進而分析市售氮化鋁粉體的ESCA圖。

English Abstract

Process development for combustion synthesis of AlN powder using Al reactant with different morphology. The reactant of experiment is different from the aluminium powder used in laboratory, the raw materials used are A-2 and A-3. A-2: The raw materials used are the 75 μm flaky aluminium powder, using programmble temperature and humidity chamber to take the surface treatment of aluminium powder. A combustion synthesis reaction was ignited by heating and lead air to fire, produce AlN under the appropriate reaction condition, the conversion ratio of product is in above 99. A-3: 15 ~ 85 μm gray irregular particle form aluminium powder, added with aluminium nitrogen process a combustion synthesis reaction, then produce AlN. The conversion ratio of product is 97.97. It is APS, GPS and phosphoric acid to take the nitrogen aluminium powder surface treatment used in the laboratory, analyze its ESCA picture, and then analyze ESCA picture of the commercial aluminium nitrogen powder.

Topic Category 工學院 > 化學工程學系
工程學 > 化學工業
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Times Cited
  1. 許倍華(2011)。氮化鋁粉體的表面改質技術開發。成功大學化學工程學系學位論文。2011。1-95。