奈米導電膠在環氧樹脂基材之製備與性質研究

黃柏源

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奈米導電膠在環氧樹脂基材之製備與性質研究

Preparation and Characterization of the Nano-clay/Polyaniline Hybrids in Epoxy Resin Matrix

黃柏源 , Masters　　Advisor：蔡宗燕　　

繁體中文

聚苯胺；環氧樹脂；黏土； Epoxy ； Clay ； Polyaniline

Abstract │ Reference (68) │ Altmetrics

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Abstract
Polyaniline  has been attracted considerable interest because of  its electric conduction、low cost and simple processing and so on.  In this work, polyaniline-modified clay hybrids in the epoxy matrix were studied. Some potential advantages are expected, such as preventing a short circuit of the electronic product、antistatic、resisting an electromagnetic wave, etc.  These kinds of protective materials have potential application in commercial markets.  The smaller, thinner and lighter electronic products are easily interfered by the electronic noise which comes from electrostatic discharge and electromagnetic interference, etc.   This noise will cause the short circuit of the electronic device.  Therefore protective materials provide the prevention of the short circuit of the electronic device in the process of preparation, transportation, storage and usage.
In this research, organically modified clays are prepared and then followed by polymerization with aniline monomer to make PANI/Clay hybrid which provide the electric conductivity.  After that, mix with epoxy resin.  Comparison of clay types, conductivity of polyaniline doped with small proton acid and/or large proton acid, and conductivity of epoxy-polyaniline/clay nanocomposites. Molecular weight of polyaniline/clay nanocomposites was measured by GPC. Finally, apply XRD, TEM, TGA and DMA measurements to observe the thermal and mechanical properties.

Reference ( 68 ) 〈TOP〉

3. 陶維屏、陳家榮，『兩岸礦產』，中華民國陶業研究學會會刊，第二十卷，第四期，p12-22.
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4. 『奈米化學與科技應用』，工業技術研究院化學工業研究所，2004.
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5. D.C. Lee, L.W. Jang，“Preparation and Characterization of PMMA-clay hybrid composite by emulsion polymerization”，J. Appl. Polymer. Sci，Vol 61，p1117-1122，1996.
連結：
6. T. Agag, T. Koga, T. Takeichi，“Studies on thermal and mechanical properties of polyimide-clay nanocomposites”，Polymer，Vol 42，p3399-3408，2001.
連結：
7. A. Gu, S. W. Kuo, F. C. Chang，“Syntheses and properties of PI/clay hybrids”，J. Appl. Polymer. Sci，Vol 79，p1902-1910，2001.
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