使用不同形態之鋁粉以燃燒合成法製備氮化鋁粉體之製程開發及反應機構探討

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使用不同形態之鋁粉以燃燒合成法製備氮化鋁粉體之製程開發及反應機構探討

Process Development for Combustion Synthesis of Aluminum Nitride Using Aluminum Powders with Different Morphology and Study on the Reaction Mechanism

陳煥煜 , Masters　　Advisor：鍾賢龍　　

繁體中文

燃燒合成法；氮化鋁； Combustion synthesis ； Aluminum Nitride

Abstract │ Reference (30) │ Times Cited (4) │ Altmetrics

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The technique for synthesis of aluminum nitride powder by self-propagating high temperature synthesis (SHS) has been well developed in our laboratory. The mostly used aluminum powder for the synthesis has been sphere in shape with dimensions of 30~80 μm, and a purity of 99.9 %. This aluminum powder has a high purity and a good reactivity but is relatively costly. In order to reduce the production cost and avoid the monopolization of source of aluminum powder, we searched for other sources for aluminum powder. Two different types of aluminum powder were investigated for synthesis of aluminum nitride: (1) irregular particle, 10~50 μm on average and 99.0 % purity; (2) irregular particle, 10~30 μm and 99.5 % purity. Previous studies indicate that these two type of aluminum powder can easily form aggregates during synthesis reaction and oxygen contents of the products are high. This thesis research focused on synthesis of aluminum nitride powder by using the aluminum powder with 10~50 μm in size, and the results were compared with experimental results of other aluminum powders. The combustion phenomena were found to be related to different surface modification of the aluminum powders, and the results were also proved by SEM observation. Beside, the poor reactivity due to high packing density of the aluminum powder was improved by setting an porous aluminum tube in the reactant compact. Using the aluminum powder and the synthesis technique developed in the present study, the product has an oxygen content of 0.3~0.6 wt% before milling, and about 1.4 wt% after milling.

Reference ( 30 ) 〈TOP〉

7. F. Miyashiro, N. Iwase, A. Tsuqe, and F. Ueno, “High thermal conductivity aluminum nitride ceramic substrates and packages”, Transactions on Components, Hybrids, and Manufacturing Technology, Vol.13, No.2, pp.313-319(1990).
連結：
8. G. Selvaduray and L. Sheet, “Aluminum nitride-review of synthesis methods”, Materials Science and Technology, Vol.9, pp.463-473 (1993).
連結：
9. F.J.-H. Haussonne, “Review of the synthesis methods for AlN”, Materials and Manufacturing Process, Vol.10, No.4, pp.717-775(1995).
連結：
11. J.F. Crider, “Self-propagating High Temperature Synthesis-A Soviet Method for producing Ceramic Materials”, in Procrrdings of the 6th Annual Conference on Composites and advances Ceramic Materials: Ceramic Engineering and Science Proceedings, Vol.3, p.519(1982).
連結：
12. S. Kumar, “Self-propagating high temperature synthesis of refractory nitrides, carbides and borides”, Key Engineering Materials, Vol. 56-57,pp.183-188(1991).
連結：

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