以化學鍍鎳表面修飾的奈米碳管應用在高分子樹脂的研究

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以化學鍍鎳表面修飾的奈米碳管應用在高分子樹脂的研究

Study of Polymer Resin Blended with Electroless Nickel Decorated Carbon Nanotubes

高祺展 , Masters　　Advisor：陳炳宏　　

繁體中文

無電鍍；鎳；碳管；導電複合材料； conductive composite film ； electroless deposition ； arbon nanotube ； nickel

Abstract │ Reference (36) │ Times Cited (1) │ Altmetrics

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Fabrication and characteristics of polymer resin blended with carbon nanotubes (CNT) decorated with electroless nickel were attempted in this work to give an economic method to produce polymer conductive composites. Carbon nanotubes are inclined to agglomerate due to their high surface energy. Hence, before nickel could be electrolessly deposited onto CNT surface, it is necessary that surface modification on CNTs, commonly in severe acidic environment, has to be undertaken priorly to render active sites that nickel can be deposited subsequently. Instead of acidic treatment, a safe and convenient method using PVP and ultrasonification was found to be able to fulfill the function. Effects of concentration, deposition time and temperature on resulted electroless nickel decorated CNT (Ni-CNT) were investigated as well. The phosphorus content of these electroless nickel alloys is about 2 ~ 3 wt%. Owing to magnetism of nickel, the Ni-CNT appeared preferably with a 1D-order orientation. Magnetic hysteresis was measured by VSM, which revealed the saturation magnetization and remnant magnetization are around 15 and 2.5 emu/g sample. The acrylic resin and epoxy resin were used in preparing polymer conductive composites. It was found that the surface resistivity is still as high as 109 Ω/sq, when matrix is acrylic resin, and lowered to 4.9×105 Ω/sq, when 9 wt% of Ni-CNT were blended with epoxy resin.

Reference ( 36 ) 〈TOP〉

Ang L-M, Hor TSA, Xu G-Q, Tung C-H, Zhao S, Wang JLS. Electroless plating of metals onto carbon nanotubes activated by a single-step activation method. Chem Mater. 1999;11:2115–2118.
連結：
Bal S, Samal SS. Carbon nanotube reinforced polymer composites–A state of the art. Bull Mater Sci. 2007;30:379–386.
連結：
Charbonnier M, Romand M. Tin-free electroless metallization of glass substrates using different PACVD surface treatment processes. Surf Coat Technol. 2002;162:19–30.
連結：
Chen BH, Hong L, Ma Y, Ko TM. Effects of surfactants in an electroless nickel-plating bath on the properties of Ni-P alloy deposits. Ind Eng Chem Res. 2002;41:2668–2678.
連結：
Chen H, Jacobs O, Wu W, Rüdiger G, Schädel B. Effect of dispersion method on tribological properties of carbon. Polym Test. 2007;26:351–360.
連結：

Times Cited (1) 〈TOP〉

蕭立羽(2009)。以化學鍍方法在奈米碳管上沉積鎳合金。成功大學化學工程學系學位論文。2009。1-70。

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