硫化銀奈米粒子/氧化鋅奈米線複合結構之製備及其應用於太陽能電池之研究

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硫化銀奈米粒子/氧化鋅奈米線複合結構之製備及其應用於太陽能電池之研究

Formation of Ag2S Nanoparticle/ZnO Nanowire Composites For Use In Solar Cells

張如君 , Masters　　Advisor：吳季珍　　

繁體中文

氧化鋅；太陽能電池；硫化銀；聲化學方法； ZnO ； Ag2S ； sonochemical method ； solar cell

Abstract │ Reference (111) │ Altmetrics

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The influences of the Au- and Pt-precoated layer on pulsed current electrodeposition of ZnO nanorods on ITO substrates have been investigated using electroanalyting methods. Compared to Pt-precoated and bare ITO substrates, the Au-precoated ITO substrate has less charging current and more positive potential than that of H2 formation in the nucleation stage at a current density of -2mAcm-2. High-density ZnO nanorods are therefore deposited on the Au-precoated ITO substrate. The Ag2S nanoparticles (NPs) have been successfully prepared on ZnO nanowires (NWs) using sonochemical method to form Ag2S NP/ZnO NW composites. XRD and TEM characterizations show that Ag2S NPs are monoclinic structure and ZnO NWs sustain single crystalline wurtzite structure after the sonochemical growth of Ag2S NPs. The proposed mechanism for Ag2S NP formaiotn is ion exchanges of ZnO NWs. Optical analyses show that the absorption wavelength of Ag2S NP is getting longer as the size increases. The solar cells are fabricated using Ag2S NP/ZnO NW composites as the photoanodes. A photoelectrochemical-cell efficiency of 0.49% is achieved using the photoanode of Ag2S NP/ZnO NW composite. Moreover, a solid solar cell composed of the Ag2S NP/ZnO NW composite with a hole conducting layer of CuSCN is also fabricated. An efficiency of 0.03% is obtained.

Reference ( 111 ) 〈TOP〉

[02] M. Grätzel, “Powering of planet”, Nature, 403, 363 (2000)
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[04] 溫慧怡，高長寬比氧化鋅奈米柱之生成－氫氣後處理效應研究，成功
連結：
[05] Z. W. Pan, Z. R. Dai, and Z. L. Wang, ”Nanobelts of semiconducting
連結：
Oxides”, Science, 291, 1947 (2001)
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[06] Y. C. Kong, D. P. Yu, B Zhang, W. Fang, and S. Q. Feng, ”Ultraviolet-emitting ZnO nanowires synthesized by a physical vapor deposition approach”, Appl. Phys. Lett., 78, 407 (2001)
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