氮化鋁粉體噴霧造粒與微波燒結製程技術開發

田瑞浦

doi:10.6844/NCKU.2012.00746

3.232.129.123，Hello！

Close
Search Quick Search Advanced Search Publication Search	Personal Service Member Login Searching History Use Bonus Card SYMSKAN
Browse Browse by University of Graduate Thesis Browse by Pinyin of Graduate Thesis Browse by Conference Proceedings Topic Browse by Conference Proceedings Publisher Browse by Pinyin of Conference Proceedings Browse by eBook Category Browse by eBook Topic Browse by eBook Publisher
Customer Services Authorize Airiti Recommend a Journal

Search Symbol (Half-width)	Description of Search Symbols
Space	"AND" indicates the intertwining of key terms used in a search
Double Quotation Marks ("") ( " " )	Double quotation marks indicate the beginning and end of a phrase, and the search will only include terms that appear in the same order of those within the quotations. Example: "image process" ： " image process "
?	Indicates a variable letter. Entering two ? will indicate two variable letters, and so on. Example: "Appl?", search results will yield apple, apply… e , appl y … ( (often used to English word searches) )
*	Indicates an unlimited number of variable letters to follow, from 1~n. Example: Enter "appl*", search results will yield apple, apples, apply, applied, application…(often used in English word searches) e , appl es , appl y , appl ied , appl ication … ( (often used to English word searches) )
AND、OR、NOT	Boolean logic combinations of key words is a skill used to expand or refine search parameters. (1) AND (1) AND: Refines search parameters (2) OR (2) OR: Expands search parameters (3) NOT: Excludes irrelevant parameters

DOI stands for Digital Object Identifier （ D igital O bject I dentifier ） ,
and is the unique identifier for objects on the internet. It can be used to create persistent link and to cite articles.

Using DOI as a persistent link

To create a persistent link, add「http://dx.doi.org/」「 http://dx.doi.org/ 」 before a DOI.
For instance, if the DOI of an article is 10.5297/ser.1201.002 , you can link persistently to the article by entering the following link in your browser: http://dx.doi.org/ 10.5297/ser.1201.002 。
The DOI link will always direct you to the most updated article page no matter how the publisher changes the document's position, avoiding errors when engaging in important research.

Cite a document with DOI

When citing references, you should also cite the DOI if the article has one. If your citation guideline does not include DOIs, you may cite the DOI link.

DOIs allow accurate citations, improve academic contents connections, and allow users to gain better experience across different platforms. Currently, there are more than 70 million DOIs registered for academic contents. If you want to understand more about DOI, please visit airiti DOI Registration （ doi.airiti.com ）。

Data Source

College of Engineering > Department of Chemical Engineering
Engineering > Chemical Industry

Bibliography Management Tool

Related Links

Report an Issue

Purchase Single Articles

Download PDF

氮化鋁粉體噴霧造粒與微波燒結製程技術開發

Process development for spray granulation and microwave sintering of aluminum nitride powder

田瑞浦 , Masters　　Advisor：鍾賢龍　　

繁體中文 DOI： 10.6844/NCKU.2012.00746

氮化鋁；噴霧造粒；微波燒結； AlN ； spray granulation ； microwave sintering

Abstract │ Reference (46) │ Altmetrics

Abstract 〈TOP〉

Parallel Abstract 〈TOP〉

In order to improve the flowability of powder, the spray granulation technique of aluminum nitride(AlN) powder was researched. Due to the advantages of microwave fast heating and energy-saving, the study explored the aluminum nitride powder by microwave sintering. At first, the study discussed the factors that the influences on the appearance of the granulation powder and particle size, such as slurry characteristics and spray granulation process parameters. And then using the single-mode microwave furnace investigated the qualities of the different granulation powder in the different soaking time. For example, shrinkage, the bulk density, secondary phase distribution, microstructure, and thermal conductivity.
The results of the experiment showed that adding ethylcellulose increased the slurry viscosity significantly and improved the hollow appearance of granulation powder. Particle size of granulation powder as the addition of binder and solid content to enhance and larger, and is inversely proportional to the rotational speed of atomizer. According to the economic effect, the study showed the results of using 2wt.% binder (B-03HX), 0.4wt.% dispersant(TEP), 0.75wt.% ethylcellulose, and 60wt.% solid content. And the thermal conductivity of the spherical granulation powder was measured 172W/m-K under the nitrogen atmosphere with a sintering temperature of 1750℃, and soaking time of 180 minutes.

Reference ( 46 ) 〈TOP〉

[1] G. A. Slack, R. A. Tanzilli, R. O. Pohl, and J. W. Vandersande, "The Intrinsic Thermal-Conductivity of Aln," Journal of Physics and Chemistry of Solids, vol. 48, pp. 641-647, 1987.
連結：
[5] 謝承佑, "高導熱氮化鋁陶瓷粉體在複合材料與電子基板應用之先導研究," 成功大學博士論文, 2006.
連結：
[7] G. L. Messing, S. C. Zhang, and G. V. Jayanthi, "Ceramic Powder Synthesis by Spray-Pyrolysis," Journal of the American Ceramic Society, vol. 76, pp. 2707-2726, Nov 1993.
連結：
[8] S. J. Lukasiewicz, "Spray-Drying Ceramic Powders," Journal of the American Ceramic Society, vol. 72, pp. 617-624, Apr 1989.
連結：
[10] K. Masters, spray drying handbook. John Wiley & Sons, Inc, 1895.
連結：

Altmetrics

〈TOP〉

E-mail ：

When an article is available to download, a notice will be sent to your mailbox address.

E-mail ：