研究芘官能化之聚氧代氮代苯并環已烷通過超分子作用力製備多面體聚矽氧烷與奈米碳管之奈米複合材料

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研究芘官能化之聚氧代氮代苯并環已烷通過超分子作用力製備多面體聚矽氧烷與奈米碳管之奈米複合材料

Investigation of POSS/CNTs Nanocomposite with Pyrene-functionalized Polybenzoxazine via Supramolecular Interaction

謝峻誠 , Masters　　Advisor：郭紹偉　　

繁體中文

混摻；單壁奈米碳管；氫鍵作用力；芘；奈米複合材料；多面體矽氧烷寡聚物；聚氧代氮代苯并環己烷； Nanocomposite ； Hydrogen bonding ； Pyrene ； single-walled carbonnanotubes ； Dispersion ； Benzoxazine ； Blend

Abstract │ Reference (52) │ Altmetrics

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In this study, we synthesized a new benzoxazine compound (Py-Bz-T), which was prepared from Py-Bz-OH for two steps reaction. 1H and 13C nuclear magnetic resonance spectroscopy (NMR) and Fourier transform infrared spectroscopy (FTIR) was used to confirm the chemical structure. Differential scanning calorimetry (DSC) and FTIR were used to investigate the curing behavior of Py-Bz-T. Thermal gravimetric analyzer (TGA) and dynamic mechanical analysis (DMA) were used to investigate the thermo properties. The import of thymine functional group increased the physical cross-linking density and better thermal properties. Ultraviolet/Visible Spectrophotometer (UV/Vis) and Photoluminescence (PL) were used to investigate the optical properties.
  First, we prepared Py-Bz-T/OBA-POSS and Py-Bz-T/SWCNTs nanocomposite. NMR and FT-IR were used to investigate the hydrogen bonding interactions of adenine (A) and thymine (T). Wide angle X-ray scattering (WAXD) was used to investigate the phase behavior. For Py-Bz-T/SWCNTs nanocomposite, PL and TGA were used to investigate optical and thermal behavior. Furthermore, we prepared Py-Bz-T/OBA-POSS/SWCNTs nanocomposite. Nanocomposite was dispersed in THF by the Transmission Electron Microscope (TEM) examination. PL, DSC and TGA were used to investigate optical and thermal behavior of Py-Bz-T/OBA-POSS/SWCNTs nanocomposite.

Reference ( 52 ) 〈TOP〉

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2. Ning, X.; Ishida, H. J. Polym. Sci. Polym. Chem.1994, 32, 1121.
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4. Wang, C. F.; Su, Y. C.; Kuo, S. W.; Huang, C. F.; Sheen, Y. C.; Chang, F. C. Angew. Chem. Int .Ed. 2006, 45, 2248.
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9. Li, X.;Gu, Y. Polym. Chem. 2011, 2, 2778.
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