Vegetables serve as an important source of natural antioxidants owing to the presence of phenolic compounds, which provide health benefits. In this study, we investigated the effect of steam-cooking on the total phenolic contents (TPC) and antioxidant activity, as assessed by oxygen radical absorbance capacity (ORAC), in sweet potato leaves (SPL) and carrots (CA). The results revealed an increase in TPC and antioxidant activity in the steamed stems and leaves of SPL. However, while TPC and antioxidant activity increased in the steamed peel of CA, there was a slight decrease in the steamed flesh of CA. A positive correlation was observed between TPC and antioxidant activity. According to the study, it is suggested that employing a suitable steam-cooking process could serve as a preferable method to enhance or preserve the TPC and antioxidant activity of SPL and CA. Further research is needed to elucidate the role of individual bioactive components influencing the antioxidant properties of SPL and CA.