- 期刊
飲料中古柯鹼檢驗方法之探討
Gas Chromatographic Method for Detection Cocaine in Beverage
摘要
較常用於古柯鹼定量之方法，為高效液相層析法和氣相層析法兩種，比較此兩儀器對古柯鹼標準品之最低檢出量分別為100ng及4ng，故採用氣相層析儀分析之。又前處理時pH值及有機溶媒的選擇也影響著回收結果，添加標準品溶液於樣品中，使其最終濃度為0.2, 0.5及1.0ppm，各濃度分別作三重覆，其平均回收率為82.8%, 55.2％及88.1%，總平均回收率為85.4%，由結果顯示本檢驗方法可用於飲料中古柯鹼含量之檢驗，而其最低檢出量為0.05ppm。
關鍵字
無資料並列摘要
A GC method was firstly compared with HPLC for cocaine content in a soft drink. The result indicated that the GC possessed higher sensitivity for cocaine hydrochloride. Its detecting limit was 4ng compared to 100ng by HPLC. Therefore the GC method was used in the further study. The cocaine solution were added to a soft drink at the final concentrations of 0.2, 0.5 and 1. ppm, the cocaine recoveries in the average of triplicate were 82.8, 85.2 and 88.1% respectively. The total average recovery was 85.0%. the cocaine recovery was especially influenced by the conditions of pH and solvent during extration. The present GC method for cocaine showed a detection limit at 0.05ppm.
並列關鍵字
無資料延伸閱讀
- 李蕙芳、鄭秋真、周薰修（1993）。市售飲料中咖啡因含量檢驗方法之探討與調查。藥物食品檢驗局調查研究年報，()，257-264。https://doi.org/10.6946/ASRNL.199309.0257
- 陳敏雄、林端著、楊仕喜、周薰修（1988）。市售飲料中古柯鹼及奎寧之調查。藥物食品檢驗局調查研究年報，()，178-179。https://doi.org/10.6946/ASRNL.198809.0178
- 洪甄敏、吳白玟、林汝青、高雅敏、曾素香、王德原（2021）。食品中羥基檸檬酸之檢驗方法探討。食品藥物研究年報，(12)，51-61。https://www.airitilibrary.com/Article/Detail?DocID=22195718-202112-202203150022-202203150022-51-61
- 蔡祈民、郭景豪、陳欣郁、林雅姿、高雅敏、曾素香、王德原（2020）。飲料中防腐劑多重檢驗方法之建立。食品藥物研究年報，(11)，47-54。https://www.airitilibrary.com/Article/Detail?DocID=22195718-202012-202101210008-202101210008-47-54
- 柳家瑞、簡俊生（2007）。Mass Spectrometry Application in Drug Abuse Control。化學，65(2)，145-150。https://doi.org/10.6623/chem.2007016