中藥之農藥殘留檢驗（VII）

Survey on Organochlorine Pesticide Residues in Raw Materials of Traditional Chinese Medicines (VII)

陳儀驊(Yi-Hua Chen) ； 徐雅慧(Ya-Hui Hsu) ； 劉宜祝(Yi-Chu Liu) ； 羅吉方(Chi-Fang Lo)

《食品藥物研究年報》 2期 (2011/12) Pp. 323-334

https://doi.org/10.6945/ARFDR.201112.0325

摘要

中藥材農藥限量標準係中藥品質管制重要規範之一，本計畫以氣相層析儀／電子捕捉偵測器（GC／ECD）、氣相層析儀／脈衝式火焰光度偵測器（GC／PFPD）、氣相層析質譜儀（GC／MS）及高效能液相層析串聯質譜儀（LC／MS／MS）進行山藥、芎藭（川芎）、甘草、白芍、熟地黃、決明子、大棗（紅棗）、苦杏仁、茯苓、陳皮、黃耆及當歸12種中藥材中acephate等215種農藥殘留量調查。結果顯示，12種中藥材，每品目各20件，共240件檢體中，陳皮14件、芎藭（川芎） 8件及大棗（紅棗）7件檢體檢出農藥殘留，其餘山藥等9種藥材均未檢出。本計畫結果提供行政管理單位作為制定管制標準之參考依據。

關鍵字

中藥材 ； 農藥殘留

並列摘要

The evaluation of pesticide residues in raw materials of traditional Chinese medicines (TCM) is essential for the quality control of TCM. In this study, the contents of pesticides in 12 raw materials of TCM, including as Dioscoreae Rhizoma, Chuanxiong Rhizoma, Glycyrrhizae Radix, Paeoniae Alba Radix, Rehmanniae Radix, Cassiae Semen, Jujubae Fructus, Armeniacae Amarum Semen, Poria, Citri Reticulatae Pericarpium, Astragali Radix and Angelicae Sinensis Radix, were investigated. Twenty samples per raw material of TCM, totally 240 samples, were tested. The residues of 215 pesticides were analyzed by GC/ECD, GC/PFPD, GC/MS and LC/MS/MS. The result showed that the organochlorine pesticide residues in all 240 samples complied with the limit. However, 14 samples of Citri Reticulatae Pericarpium, 8 samples of Chuanxiong Rhizoma, 7 samples of Jujubae Fructus contained pesticide residues. The results could be provided as the reference for the regulatory authority.

並列關鍵字

traditional Chinese medicines ； pesticide residue