The experiment produced composite coating with Ni-base material ingredient and different TiO2 concentration, stirring rate of electrolyzed commercial pure titanium formed TiO2 particles into the electrolyth bath which was used distinct direct or pulse current density, then analyzing the coating of TiO2 particles contents, surface morphology and structure to the effects of microhardness and corrosion resistance. As a result, we found microhardness and corrosion resistance will increase. The result was that TiO2 particles in the composite coatings increasing with average content. Besides, the advantages of the process was using electrolysis could dispersed TiO2 particles into the Electroplating solution with easily change to the particles content and properties. The most important thing was saving the cost of process. Therefore, it will increase the capability of competition in composite plating industry.