The interferometric zone plate is the essential of HOEs, which is the interference between plane wave and sphere wave, can focus the light beam by diffraction, instead of the way which conventional lens or concave mirrors do. In view of the concentration, the simple zone plate can’t meet all needs of its function. Since the dichromated gelatin has a higher diffraction efficiency in all holographic recording materials, the aim of this research is to use dichromated gelatin as the recording material and to make use of the principle of holography to design holographic optical components, especially in fabrication procedure of dichromated gelatin film and in experimental technique to form a high diffraction efficiency using different angular exposure method.