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真空預燒結製備Pb(Mn_(1/3)Nb_(2/3))O_3-PZ-PT陶瓷

The Study on Pb(Mn_(1/3)Nb_(2/3))O_3-PZ-PT Piezoelectric Ceramics Pre-sintered in Vacuum

摘要


本實驗是利用真空預燒結的方式將0.07PMnN-0.468PZ-0.462PT壓電陶瓷的緻密性提升,並在800℃下破真空以空氣氣氛燒結避免大量的鉛揮發的產生。由室溫抽真空並加溫至800℃破真空後直接升溫至1050℃持溫1小時有最佳的壓電特性與相對密度的表現,此時的Qm可達2050且k_p亦可維持在0.613。有真空預燒結的製程在燒結溫度方面有明顯的下降,且較傳統燒結流程下降約150℃。

關鍵字

真空燒結 PZT

並列摘要


Pre-sintering in vacuum was used to enhance the densification of sintered 0.07PMnN-0.468PZ-0.462PT ceramics in this study. This pre-sintering process was to heat the samples from room temperature to 800°C under 10^(-2) torr vacuum condition. When temperature reaches 800°C, air with ambient pressure is conducted into the chamber, in the mean time, the samples were continuously heated to 1050°C for various holding periods. In the case of holding 1 hour, best combination piezoelectric properties of this ceramics were obtained, where Qm and k_p was 2050 and 0.613 respectively. Comparing with conventional sintering process, this pre-sintering process can lower sintering temperature up to 150°C without deteriorating piezoelectric properties of these ceramics.

並列關鍵字

Vacuum sinteringm PZT

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