以線上淨化高效離子層析法分析食品中溴酸鹽

Determination of Bromate Amounts in Foods by High Performance Ion Chromatography Using On-line Solid Phase Extract

蔡佳芬(Chia-Fen Tsai) ； 方銘志(Ming-Chih Fang) ； 曾仁鴻(Jen-Hung Tseng) ； 潘志寬(Jyh-Quan Pan) ； 施養志(Daniel Yang-Chih Shih)

《食品藥物研究年報》 1期 (2010/11) Pp. 1-4

https://doi.org/10.6945/ARFDR.201011.0001

摘要

High performance ion chromatography (HPIC) with suppressed conductivity detector was developed for the analysis of bromate content in foods in this study. Bromate was extracted from foods using deionized water. Two sets of IonPac AS9-HC (4 mm)+IonPac AG9-HC (4 mm) columns were connected and used for the clean up and separation, while 9 mM Na2CO3 solution was used as mobile phase in HPIC. It was a simple, quick and solvent-saving method for the analysis, the recoveries of bromate spiked in wheat flour and bread (50 ppb), cookies (200 ppb) were all above 90%. All of 11 various cookies and potato chips purchased in Taipei were not detected for bromate by this method.

關鍵字

溴酸鹽 ； 高效離子層析儀 ； 麵粉 ； 麵包 ； 餅乾

並列摘要

High performance ion chromatography (HPIC) with suppressed conductivity detector was developed for the analysis of bromate content in foods in this study. Bromate was extracted from foods using deionized water. Two sets of IonPac AS9-HC (4 mm)+IonPac AG9-HC (4 mm) columns were connected and used for the clean up and separation, while 9 mM Na2CO3 solution was used as mobile phase in HPIC. It was a simple, quick and solvent-saving method for the analysis, the recoveries of bromate spiked in wheat flour and bread (50 ppb), cookies (200 ppb) were all above 90%. All of 11 various cookies and potato chips purchased in Taipei were not detected for bromate by this method.

並列關鍵字

bromate ； high performance ion chromatography ； wheat flour ； bread ； cookies